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State of the Art of Microreaction Technology |
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1 | (14) |
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1 | (4) |
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Microsystems Termed Microreactor |
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1 | (1) |
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Structural Hierarchy of Microreactors |
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1 | (3) |
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Functional Classification of Microreactors |
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4 | (1) |
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Dividing Line Between Analysis and Reaction Systems |
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4 | (1) |
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Fundamental Advantages of Microreactors |
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5 | (5) |
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Fundamental Advantages of Miniaturized Analysis Systems |
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5 | (1) |
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Fundamental Advantages of Nano-Scale Reactors |
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5 | (1) |
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Advantages of Microreactors Due to Decrease of Physical Size |
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6 | (2) |
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Advantages of Microreactors Due to Increase of Number of Units |
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8 | (2) |
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Potential Benefits of Microreactors Regarding Applications |
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10 | (2) |
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12 | (3) |
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Modern Microfabrication Techniques for Microreactors |
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15 | (26) |
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Microfabrication Techniques Suitable for Microreactor Realization |
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15 | (1) |
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Evaluation of Suitability of a Technique |
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16 | (1) |
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Anisotropic Wet Etching of Silicon |
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17 | (2) |
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19 | (1) |
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20 | (1) |
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21 | (1) |
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Wet Chemical Etching of Glass |
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22 | (1) |
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Advanced Mechanical Techniques |
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23 | (2) |
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Surface Cutting with Diamond Tools |
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23 | (1) |
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Milling, Turning and Drilling |
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23 | (1) |
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24 | (1) |
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24 | (1) |
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Isotropic Wet Chemical Etching of Metal Foils |
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25 | (1) |
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Electro Discharge Machining (EDM) of Conductive Materials |
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26 | (3) |
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Wire-Cut Erosion and Die Sinking |
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27 | (2) |
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29 | (1) |
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29 | (1) |
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Interconnection Techniques |
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30 | (3) |
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Microlamination of Thin Metal Sheets |
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30 | (3) |
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33 | (2) |
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Functional Coatings for Corrosion Prevention |
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33 | (1) |
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Functional Coatings for Fouling Prevention |
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34 | (1) |
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35 | (6) |
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41 | (46) |
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Mixing Principles and Classes of Macroscopic Mixing Equipment |
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41 | (2) |
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Mixing Principles and Classes of Miniaturized Mixers |
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43 | (3) |
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Potential of Miniaturized Mixers |
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46 | (3) |
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Contacting of Two Substreams, e.g. in a Mixing Tee Configuration |
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49 | (3) |
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Mixing Tee-Type Configuration |
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49 | (1) |
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Double Mixing Tee-Type Configuration |
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50 | (2) |
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Collision of High-Energy Substreams for Spraying/Atomizing |
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52 | (1) |
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Collision of Three Substreams in a Microjet Reactor |
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52 | (1) |
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Injection of Many Small Substreams of One Component into a Main Stream of Another Component |
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53 | (2) |
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Injection of Multiple Microjets |
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53 | (2) |
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Manifold Splitting and Recombination of a Stream Consisting of Two Fluid Lamellae of Both Components |
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55 | (9) |
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Multiple Flow Splitting and Recombination Combined with Channel Reshaping |
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55 | (3) |
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Multiple Flow Splitting and Recombination Using Fork-Like Elements |
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58 | (2) |
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Multiple Flow Splitting and Recombination Using a Separation Plate |
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60 | (2) |
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Multiple Flow Splitting and Recombination Using a Ramp-Like Channel Architecture |
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62 | (2) |
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Injection of Many Substreams of Both Components |
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64 | (16) |
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Multilamination of Fluid Layers in an Interdigital Channel Configuration |
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64 | (9) |
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Vertical Multilamination of Fluid Layers Using a V-type Nozzle Array |
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73 | (2) |
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Multilamination Using a Stack of Platelets with Microchannels |
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75 | (4) |
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Multilamination Using a Stack of Platelets with Star-Shaped Openings |
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79 | (1) |
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Decrease of Diffusion Path Perpendicular to the Flow Direction by Increase of Flow Velocity |
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80 | (3) |
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Decrease of Layer Thickness by Hydrodynamic Focussing |
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80 | (3) |
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Externally Forced Mass Transport, e.g. by Stirring, Ultrasonic Wave, Electrical and Thermal energy |
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83 | (1) |
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Dynamic Micromixer Using Magnetic Beads |
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83 | (1) |
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83 | (4) |
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87 | (28) |
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Micro Heat Exchangers with Wide and Flat Channels |
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89 | (10) |
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Cross-Flow Heat Exchange in Stacked Plate Devices |
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89 | (3) |
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Cross-Flow Heat Exchange Based on Cross-Mixing |
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92 | (2) |
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Counter-Flow Heat Exchange in Stacked Plate Devices |
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94 | (3) |
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Electrically Heated Stacked Plate Devices |
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97 | (2) |
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Micro Heat Exchangers with Narrow and Deep Channels |
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99 | (3) |
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Heat Exchanger with One-Sided Structured Channels |
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99 | (1) |
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Heat Exchanger with Double-Sided Structured Channels |
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100 | (2) |
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Micro Heat Exchangers with Breakthrough Channels |
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102 | (2) |
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104 | (2) |
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Numerical Calculations of the Influence of Material Choice on Heat Transfer Efficiency |
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104 | (1) |
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The Use of Thermal Blocking Structures |
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105 | (1) |
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Permanent Generation of Entrance Flow by Fins |
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106 | (1) |
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Generation of a Periodic Flow Profile by Sine-Wave Microchannels |
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107 | (1) |
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Microtechnology-Based Chemical Heat Pumps |
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108 | (1) |
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Performance Characterization of Micro Heat Exchangers |
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109 | (3) |
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Temperature Profiles of Micro Heat Exchangers Yielded by Thermograms of Infrared Cameras |
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110 | (2) |
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112 | (3) |
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Microseparation Systems and Specific Analytical Modules For Microreactors |
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115 | (28) |
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115 | (15) |
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Partially Overlapping Channels |
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115 | (4) |
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Wedge-Shaped Flow Contactor |
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119 | (3) |
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Contactor Microchannels Separated by a Micromachined Membrane |
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122 | (4) |
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Contactor Microchannels Separated by Sieve-Like Walls |
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126 | (1) |
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Micromixer--Settler Systems |
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126 | (4) |
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130 | (3) |
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Isoporous-Sieve Microfilters |
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131 | (1) |
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131 | (2) |
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Gas Purification Microsystems |
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133 | (1) |
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Gas Separation Microdevices |
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134 | (2) |
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Specific Analytical Modules for Microreactors |
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136 | (4) |
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Analytical Modules for In-Line IR Spectroscopy |
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136 | (1) |
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Analytical Module for Fast Gas Chromatography |
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136 | (4) |
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140 | (3) |
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Microsystems for Liquid Phase Reactions |
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143 | (30) |
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Types of Liquid Phase Microreactors |
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144 | (1) |
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Liquid/Liquid Synthesis of a Vitamin Precursor in a Combined Mixer and Heat Exchanger Device |
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144 | (7) |
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Acrylate Polymerization in Micromixers |
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151 | (3) |
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Ketone Reduction Using a Grignard Reagent in Micromixers |
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154 | (4) |
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Laboratory-Scale Organic Chemistry in Micromixer/Tube Reactors |
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158 | (4) |
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Dushman Reaction Using Hydrodynamic Focusing Micromixers and High-Aspect Ratio Heat Exchangers |
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162 | (2) |
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Synthesis of Microcrystallites in a Microtechnology-Based Continuous Segmented-Flow Tubular Reactor |
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164 | (2) |
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Electrochemical Microreactors |
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166 | (5) |
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Synthesis of 4-Methoxybenzaldehyde in a Plate-to-Plate Electrode Configuration |
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166 | (3) |
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Scouting Potentiodynamic Operation of Closed Microcells |
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169 | (2) |
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171 | (2) |
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Microsystems for Gas Phase Reactions |
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173 | (51) |
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Catalyst supply for Microreactors |
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173 | (3) |
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Types of Gas Phase Microreactors |
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176 | (1) |
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Microchannel Catalyst Structures |
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177 | (16) |
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Flow Distribution in Microchannel Catalyst Reactors |
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177 | (1) |
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Partial Oxidation of Propene to Acrolein |
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178 | (2) |
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Selective Partial Hydrogenation of a Cyclic Triene |
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180 | (4) |
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184 | (2) |
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Selective Partial Hydrogenation of Benzene |
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186 | (1) |
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Selective Oxidation of 1-Butene to Maleic Anhydride |
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187 | (1) |
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Selective Oxidation of Ethylene to Ethylene Oxide |
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187 | (1) |
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Reactions Utilizing Periodic Operation |
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188 | (5) |
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Microsystems with Integrated Catalyst Structures and Heat Exchanger |
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193 | (10) |
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Oxidative Dehydrogenation of Alcohols |
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193 | (4) |
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Synthesis of Methyl Isocyanate and Various Other Hazardous Gases |
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197 | (3) |
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H2/O2 Reaction in the Explosion Regime |
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200 | (3) |
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Microsystems with Integrated Catalyst Structures and Mixer |
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203 | (6) |
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Synthesis of Ethylene Oxide |
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203 | (6) |
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Microsystems with Integrated Catalyst Structures, Heat Exchanger and Sensors |
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209 | (8) |
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209 | (5) |
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214 | (3) |
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Microsystems with Integrated Mixer, Heat Exchanger, Catalyst Structures and Sensors |
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217 | (1) |
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HCN Synthesis via the Andrussov Process |
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217 | (7) |
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224 | (33) |
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229 | (1) |
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Gas/Liquid Contacting Principles and Classes of Miniaturized Contacting Equipment |
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229 | (15) |
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Contacting of Two Gas and Liquid Substreams in a Mixing Tee Configuration |
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232 | (1) |
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Injection of One Gas and Liquid Substream |
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232 | (1) |
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Injection of Many Gas and Liquid Substreams into One Common Channel |
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233 | (2) |
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Injection of Many Gas and Liquid Substreams into One Packed Channel |
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235 | (2) |
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Injection of Many Gas Substreams into One Liquid Channel with Catalytic Walls |
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237 | (2) |
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Injection of Many Gas and Liquid Substreams into Multiple Channels |
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239 | (5) |
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Generation of Thin Films in a Falling Film Microreactor |
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244 | (11) |
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255 | (2) |
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Microsystems for Energy Generation |
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257 | (14) |
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Microdevices for Vaporization of Liquid Fuels |
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257 | (3) |
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Microdevices for Conversion of Gaseous Fuels to Syngas by Means of Partial Oxidations |
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260 | (5) |
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Hydrogen Generation by Partial Oxidations |
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260 | (1) |
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Partial Oxidation of Methane in a Stacked Stainless Steel Sheet System |
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261 | (2) |
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Partial Oxidation of Methane in a Microchannel Reactor |
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263 | (2) |
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Microdevices for Conversion of Gaseous Fuels to Syngas by Means of Steam Reforming |
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265 | (3) |
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Steam Reforming of Methanol in Microstructured Platelets |
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265 | (3) |
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268 | (3) |
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Microsystems for Catalyst and Material Screening |
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271 | (6) |
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Parallel Screening of Heterogeneous Catalysts in a Microchannel Reactor |
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271 | (3) |
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Parallel Screening of Heterogeneous Catalysts in Conventional Mini-Scale Reactors |
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274 | (2) |
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276 | (1) |
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Methodology for Distributed Production |
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277 | (8) |
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277 | (3) |
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Miniplant Concept for HCN Manufacture |
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278 | (1) |
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The Disposable Batch Miniplant |
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279 | (1) |
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Paradigm Change in Large-Scale Reactor Design Towards Operability and Environmental Aspects Using Miniplants |
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280 | (3) |
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283 | (2) |
| Index |
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285 | |